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17 articles for “One-pot Synthesis”
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Study of the Effect of SLS Loading on the One-Pot Synthesis of Substituted Piperidines
Abstract: Piperidine derivatives represent a vital class of nitrogen-containing heterocycles with extensive pharmacological and industrial significance. Their synthesis has garnered considerable interest due to their presence in numerous bioactive molecules, including drugs with CNS activity, analgesic properties, and antimicrobial effects. Traditional multi-step synthetic pathways are often time-consuming and resource-intensive. To address this, one-pot multicomponent reactions (MCRs) have emerged as an efficient and eco-friendly alternative, allowing for the rapid construction of complex …
Published in International Journal of Green Chemistry · Vol. 12, Issue 1, 2026 · pp. 1–9 Read article
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Extracellular One Pot Green Synthesis of Palladium Nanoparticles
Abstract: Extracellular in-situ synthesis of metal nanoparticles using extracts of plants like Azadirachta indica (Neem), and Zingiber officinale (Ginger) has been successfully carried out earlier. In this study, we have developed a novel method to synthesize Palladium nanoparticles by the process of bio-chemical reaction between Palladium salt solution with seed extract of Coriandrum sativum without using any surfactant or external energy. By this method, physiologically stable, bio-compatible Pd nanoparticles (NPs) were …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 1, Issue 1, 2015 · pp. 1–7 Read article
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Zirconium tetrachloride catalyzed one-pot highly efficient green synthesis of functionalized piperidines under visible light
Abstract: AbstractHighly efficient multicomponent one-pot green synthesis of a series of pharmaceutically interesting functionalized piperidine derivatives has been developed based on a low-cost and eco-friendly zirconium tetrachloride catalyst via tandem reactions of 1,3-dicarbonyl compounds, aromatic aldehydes, and various amines in ethanol under visible light. High atom-economy, high yields, less reaction times, eco-friendly, and mild reaction conditions are some of the important features of this protocol.Key words: ZrCl4, piperidines, multi-component reactions, visible …
Published in International Journal of Green Chemistry · Vol. 6, Issue 1, 2020 · pp. 36–43 Read article
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One-Pot Multicomponent Reactions: A Versatile Approach for Heterocyclic Compound Synthesis
Abstract: Multicomponent reactions (MCRs) represent an efficient and versatile approach in organic synthesis, enabling the formation of complex molecules through a single, one-pot procedure. This methodology is particularly advantageous for the synthesis of heterocyclic compounds that are prevalent in numerous biologically active molecules and pharmaceuticals. The one-pot nature of MCRs allows for the simultaneous combination of three or more reactants, leading to high atom economy, reduced reaction times, and minimized purification …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 10, Issue 1, 2025 · pp. 1–7 Read article
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Synthesis and Characterization of Magnetite-Pectin-Alginate Hybrid and Bionanocomposite
Abstract: It is a one pot synthesis of hybrid bionanocomposite comprising of inorganic magnetite with stabilizer biopolymer pectin and alginate in co-precipitation method using sodium hydroxide and ammonium hydroxide as precipitating agents. A lot of comparison and investigation has been done in particle size of nanocomposite by changing the stoichiometric ratio of both magnetite and biopolymer concentration and drying condition of composite. The nanocomposite has been characterized using infrared spectroscopy (FTIR), …
Published in International Journal of Applied Nanotechnology · Vol. 3, Issue 1, 2017 · pp. 18–22 Read article
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General and Organic Chemistry Laboratory Experiments for Science, Pre-medical, and Pharmacy Students – Chapter V: Organic Synthesis
Abstract: Organic synthesis can be classified into many types, including simple one-step synthesis, multi-step, one-pot, microwave, or green synthesis. Each type of synthesis takes place through a specific pathway depending on reactants involved, the reaction conditions, the catalyst, the protection group, and the duration of the reaction. In some cases, the required compound can be prepared by more than one procedure, and an expert chemist prefers the procedure by which the …
Published in International Journal of Analytical and Applied Chemistry · Vol. 12, Issue 2, 2026 · pp. 8–16 Read article
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Crystal Growth, Synthesis and Characteristic Studies of Bismuth Doped Tristhioureazinc (II) Sulpate (ZTS) Crystal
Abstract: Potential semi organic tristhioureazinc(II) sulphate (ZTS), One of the best room temperature growth techniques for nonlinear optical materials with high SHG efficiency is slow evaporation solution growth, which produces pure and single crystals for use in laser technology and photonic applications. Single crystals Doping of Bismuth fluoride (equimolar) to ZTS is done during the crystallization process is further analysed by single crystal XRD which infers that the Bismuth doped ZTS …
Published in International Journal of Chemical Separation Technology · Vol. 9, Issue 2, 2023 · pp. 45–52 Read article
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Innovative Approaches to Organic and Inorganic Nanocomposite Synthesis: Chemical Reaction Pathways
Abstract: The integration of organic and inorganic nanomaterials has emerged as a prominent trend in various sectors, driven by the unique properties and functionalities that nanoscale materials offer. This study elucidates the current landscape of organic-based nanomaterials, highlighting their synthesis, characterization, and application potential across different fields. The miniaturization principle has catalyzed the development of nanocomposites that combine inorganic and organic constituents, enhancing the reactivity and performance of traditional materials through …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 10, Issue 2, 2025 · pp. 1–9 Read article
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Identifying the Age Using Face Image Using DWT, LBP, SVM and k-NN
Abstract: ABSTRACTThe research related to identifying the age using face images has become progressively more important, due to the fact it has a multiplicity of potentially helpful applications. In this paper we survey the complete age synthesis or age estimation from face images techniques. Automatic facial age identifying is one of the main issues in pattern recognition which shows the age of human according to her/his facial expressions. Basically, age detection/estimation …
Published in International Journal of Image Processing and Pattern Recognition · Vol. 6, Issue 2, 2020 · pp. 26–37 Read article
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SYNTHESIS OF BIOGAS – A REVIEW
Abstract: Energy is universally recognized as one of the most important inputs for economic growth and human development. Every day, in our walks of life we come across food, vegetable wastes and other organic wastes that have huge potential to uplift the society in a better way, when these are transformed into useful bioenergy. To produce bioenergy from biomass one of the better options is to utilize these potential wastes to …
Published in International Journal of Agrochemistry · Vol. 4, Issue 2, 2018 · pp. 59–67 Read article
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Synthesis of Zeolites: An Overview
Abstract: Zeolites are microporous, aluminosilicate minerals commonly used as commercial adsorbents and catalysts. Zeolite synthesized from CFA is a minor but interesting product, with high environmental applications. Zeolites may be easily obtained from CFA by relatively cheap and fast conversion processes. This paper provides an overview on the methodologies for zeolite synthesis from CFA, and a detailed description of conventional alkaline conversion processes, with special emphasis on the experimental conditions to …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 3, Issue 2, 2017 · pp. 8–14 Read article
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Synthesis, Crystal Growth and Characterization of Bismuth Doped Potassium Hydrogen Phthalate Crystal (Khp): A Nlo Material
Abstract: To create single crystals using the Slow Evaporation Solution Growth Technique (SEST), equimolar composition of the transition metal (Bi) as Bismuth nitrate is added to Potassium Hydrogen Phthalate (KHP) (1:1) at ambient temperature. The following analysis is then performed on the single crystals that have formed. Equimolar doping-induced structural distortion in the crystals is confirmed by the FT-IR Spectra. The TGDTA study reveals the purity of the material and no …
Published in International Journal of Composite Materials and Matrices · Vol. 10, Issue 1, 2024 · pp. 19–27 Read article
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Green Nanotechnology: Innovative Approaches for Sustainable Mosquito Control – A Review
Abstract: Mosquitoes are well-known carriers of various parasites and viruses that can lead to several serious diseases in humans. Illnesses such as malaria, dengue fever, epidemic encephalitis B, and epidemic typhus are among the major health threats transmitted by these insects. Because effective vaccines are lacking for many mosquito-borne viruses (arboviruses), controlling the mosquito population remains the primary method for preventing these diseases. Unfortunately, the increasing resistance of mosquitoes to conventional …
Published in International Journal of Environmental Chemistry · Vol. 11, Issue 2, 2025 · pp. 1–8 Read article
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Design Techniques of Green Building
Abstract: The green building concept has been with successfully accepted by several countries in their construction to save the loss of energy, defend atmosphere, and recycle the materials. Green building style minimizes the negative human impacts on the natural resources. Passive star building style is one among the subcategories of the green building concept. Execution of the concept of passive star building style within the tropical countries incorporates a bigger potential …
Published in International Journal of Sustainable Building Technology · Vol. 2, Issue 1, 2019 · pp. 9–33 Read article
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Nanostructured Metal Oxides as Promising Electrode Materials for Microbial Fuel Cells
Abstract: Microbial fuel cells (MFCs) are emerging as a promising technology for generating sustainable energy from organic waste materials. One of the key challenges in developing efficient MFCs is the selection of suitable electrode materials. In recent years, nanostructured metal oxides have gainedconsiderable attention as electrode materials for MFCs due to their unique structural and electrochemical properties. This review highlights the recent progress in the development and application of various types …
Published in International Journal of Applied Nanotechnology · Vol. 8, Issue 2, 2022 · pp. 23–30 Read article
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Synthesis, Structural Elucidation, and Antimicrobial Screening of a Cobalt (II) Coordination Compound Derived from a Thiophene-Containing Schiff Base
Abstract: Abstract An N, O-chelating azomethine Schiff base ligand (HL), chemically identified as 2-{[(thiophen-2-yl) methylidene] amino} benzoic acid, was synthesized by an equimolar condensation reaction between thiophene-2-carbaldehyde and anthranilic acid in absolute ethanol in the presence of a catalytic amount of acetic acid. The corresponding cobalt (II) complex, formulated as [Co(L)₂] · 2H₂O, was prepared by refluxing two equivalents of the ligand with one equivalent of cobalt (II) acetate tetrahydrate in …
Published in International Journal of Analytical and Applied Chemistry · Vol. 12, Issue 2, 2026 · pp. 1–7 Read article
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Literature Review on Overcoming Graphene Dispersion Challenges in Ultra High Performance Concrete: A Review of Self-Dispersion and Bio-Polymer Encapsulation Strategies
Abstract: Abstract—Ultra-High-Performance Concrete (UHPC) is a new generation of cement-based material because of its higher compressive and tensile strength, increased durability, and higher resistance to environmental degradation. However, UHPC undergoes microcracking when subjected to mechanical and thermal loading, which can jeopardize the long-term performance of the structure, decrease service life, and cause expensive maintenance. Traditional solutions to enhance UHPC durability are centered on material densification and fiber strengthening, while these treatments …
Published in International Journal of Concrete Technology · Vol. 12, Issue 1, 2026 · pp. 31–46 Read article