Search
117 articles for “X-Ray”
-
Assessment of Groundwater Quality Affected by Open Dumping Site in Hyderabad Pakistan
Abstract: The present study has been conducted to evaluate the different samples of groundwater, surface leachate and Soil, for the determination of chemical parameters of surface leachate and their effects on soil using X-Ray Fluorescence spectroscopic (XRF) technique. Samples were collected from the vicinity of unregulated dumping site area of Hyderabad, Pakistan. Different chemical and elements including essential trace and toxic were determined. The impact assessment of leachate on the quality …
Published in International Journal of Environmental Chemistry · Vol. 5, Issue 1, 2019 · pp. 23–30 Read article
-
Synthesis of Nano-ZnO by Chemical Method and its Characterization
Abstract: Nanocrystals of ZnO were prepared by chemical method using Zn (II) acetate and potassium hydroxide as the starting materials and methanol as solvent. The material was characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), electron diffraction analysis (EDS), UV-Visible spectroscopy, Dynamic light scatteringanalysis (DLS) and Fourier transform spectroscopy (FTIR) techniques. The results indicated that the obtained ZnO material was in nano-dimension and possessed pure …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 1, 2022 · pp. 13–18 Read article
-
Characterization and Kinetic Study of Sugarcane Bagasse for the Production of Bio-oil Over Monodispersed Fe2 O3 and ZSM-5 Composite
Abstract: The shortage and price scramble of fossil fuels accompanied by vast CO2 emissions have triggered a worldwide search for alternative and sustainable resources. Wind, solar, geothermal, biomass, and water are the most commonly used alternative energy sources. The biomass residues are typically at low cost and readily availabile, and has been used as feedstocks for synthesis of renewable energy. To produced the bio-fuels from biomass residues, several reaction pathways categorized …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 9, Issue 2, 2023 · pp. 1–13 Read article
-
Synthesis and Characterization of Magnetite-Pectin-Alginate Hybrid and Bionanocomposite
Abstract: It is a one pot synthesis of hybrid bionanocomposite comprising of inorganic magnetite with stabilizer biopolymer pectin and alginate in co-precipitation method using sodium hydroxide and ammonium hydroxide as precipitating agents. A lot of comparison and investigation has been done in particle size of nanocomposite by changing the stoichiometric ratio of both magnetite and biopolymer concentration and drying condition of composite. The nanocomposite has been characterized using infrared spectroscopy (FTIR), …
Published in International Journal of Applied Nanotechnology · Vol. 3, Issue 1, 2017 · pp. 18–22 Read article
-
Bioethanol Production from Corncob Cellulosic Biomass: RSM and ANN based Optimization for Dilute Acid Pretreatment
Abstract: To increase the yield of fermentable sugars, the complexity of lignocellulosic biomass requires a pretreatment method. Dilute acid hydrolysis was used to efficiently pretreatment corn cobs. The aim of this study was to characterize corncob and investigate the effect of process parameters on total reducing sugar (TRS) yield during dilute acid hydrolysis pretreatment of corncob biomass. The morphology and microstructure of the samples were examined using an X-ray diffraction machine, …
Published in International Journal of Chemical Engineering and Processing · Vol. 9, Issue 2, 2023 · pp. 16–34 Read article
-
Hazardous Effect of Radioactive Pollution on Environment and Their Possible Preventive Measures
Abstract: Radioactive pollution is the release of radioactive substances or high-energy particles into the air, water, or earth as a result of human activity, either by accident or by design. Radioactive contamination, also called radiological contamination, is the deposition of, or presence of radioactive substances on surfaces or within solids, liquids or gases (including the human body), where their presence is unintended or undesirable (from the International Atomic Energy Agency - …
Published in International Journal of Environmental Chemistry · Vol. 3, Issue 2, 2017 · pp. 19–25 Read article
-
Effect of Sulphamic acid on the growth of Glycine single crystals
Abstract: Sulphamic acid added glycine single crystals were grown successfully by slow-evaporation technique.A single crystal with well defined crystal was obtained. The lattice parameters and crystal system of the grown crystals were confirmed by single crystal and powder x-ray diffraction analysis.The functional groups present in the sample were identified by FTIR spectral analysis.The lower cut off wavelength and bandgap energy of the grown crystal was analysed from uv-vis spectral analysis. Keywords: …
Published in International Journal of Energetic Materials · Vol. 5, Issue 1, 2019 · pp. 9–13 Read article
-
Low Temperature Chemical Synthesis of Nickel Oxide Microflower and Study of its Optical and Thermal Properties
Abstract: A simple rout for the synthesis of flower like nickel oxide nanostructure has been reported using nickel sulphate and potassium per-sulphate as precursor. Efforts were made to see the effect of persulfate amount on different properties of the materials thus two samples were synthesized with different amount of per-sulphate precursors. The as prepared samples were characterized by x-ray diffraction, field emission scanning and transmission electron microscope, thermal gravimetric and differential …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 4, Issue 2, 2018 · pp. 17–24 Read article
-
Chemical Synthesis and Characterization of Polyaniline for Supercapacitors Application
Abstract: Various polyaniline (PANI) synthesis methods are reported in the literature, depending on the experimental parameters involved (T, t, doping, and mixing procedure). Herein, three chemical polymerization methods were used to synthesis PANI from aniline monomer: rapid oxidation (OR), controlled oxidation (CO), and interfacial oxidation (OI). The PANI was therefore deposited next by drop casting on a silicon (Si) substrate. X-ray diffraction, Raman spectroscopy, and scanning electron microscopy were used to …
Published in International Journal of Chemical Engineering and Processing · Vol. 8, Issue 2, 2022 · pp. 9–16 Read article
-
Effect of Calcium doping on Structural and Morphological properties of YBCO Superconductor
Abstract: In this paper, we have reported the effect of Ca doping in YBCO superconductors with an aim of understanding the effect of novel local nano distortions on the superconducting properties of YBCO. Solid state reaction method is used to prepare the samples. X-Ray diffraction pattern shows that the samples are polycrystalline and having orthorhombic structure while Resistivity measurement shows that Tc decreases with increase in Ca-doping.Morphological studies reveals clear evolution …
Published in International Journal of Applied Nanotechnology · Vol. 6, Issue 1, 2020 · pp. 6–10 Read article
-
Mechanical Studies and Thermal Kinetics of Isoniazid Crystals
Abstract: Single crystals of isoniazid were crystallized by slow solvent evaporation method. The crystal structure was confirmed using single crystal X-ray diffraction analysis. Micro hardness was estimated and work hardening coefficient and Newtonian resistance pressure of the crystal were determined. Kinetic analysis of the thermogravimetric data was carried out by using Coats-Redfern relation. Activation energy, frequency factor and order of reaction were also calculated. Arrhenius equation for isoniazid is k=0.43×105e–79103/RT mol–1s–1. …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 1, Issue 1, 2015 Read article
-
Synthesis, Crystal growth and Characterization of Lead acetate zinc (II)Sulphate Material
Abstract: Leadacetatezinc (II) Sulphate Crystal is synthesized by the addition of Leadacetate to Zinc sulphate in equimolar concentration (1:1ratio) to produce larger sized crystal but during the crystallization process a bulk of colourless precipitate was obtained and after filtration the crystals are formed in the filtrate after slow evaporation solution growth technique. Thus formed crystals from the filtrate is kept away and the precipitate formed during the crystallization process is characterized …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 22–29 Read article
-
Synthesis of Fe2(MoO4)3/MoO3 Nanocatalysts by Solution Combustion Approach and Their Catalytic Performance for the Selective Oxidation of Methanol
Abstract: The Fe 2 (MoO 4 ) 3 /MoO 3 nanocatalysts comprising Fe 2 (MoO 4 ) 3 nanoparticles supported on MoO 3 nanorods were synthesized via two-step solution combustion approach and their catalytic performance for the selective oxidation of methanol were evaluated. The materials have been characterised using electron microscopy, powder X-ray diffraction and Raman spectroscopy. First, MoO 3 nanoparticles were prepared by solution combustion reaction employing ammonium nitrate as …
Published in International Journal of Applied Nanotechnology · Vol. 10, Issue 1, 2024 · pp. 37–47 Read article
-
Correlation for Photocatalytic Degradation Kinetics of Carboxylic Acids by Electrochemically Synthesized Cd/ZnO Nanoparticles and Study of Antibacterial Behaviour
Abstract: Cd/ZnO nanoparticle has been successfully synthesized by electrochemical method which is simple and inexpensive method. The synthesized Cd/ZnO nanoparticle was used has a catalyst for the photodegradation of Oxalic acid, Chloroacetic acid and Formic acid under various experimental conditions by volumetric method. The Cd/ZnO nanoparticles were characterized by various techniques such as SEM-EDAX, UV-Visible spectroscopy, FTIR-IR spectrum and X-ray diffraction studies. The study of UV-Visible spectroscopy revealed that the Cd/ZnO …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 6, Issue 2, 2020 · pp. 1–16 Read article
-
Characterization and Wear Behavior of TiN, TiAlN, TiCrN and AlCrN PVD Coatings Deposited onto AISI H13 Hot Forging Die Steel
Abstract: Four Nitride coatings TiN, TiAlN, TiCrN and AlCrN were deposited onto AISI H13 hot work die steel by cathodic arc evaporation physical vapour deposition (PVD) technique. The coatings were characterized by SEM, SEM-EDS, XRD, line scan EDS and X-Ray mapping tests and micro hardness tester. The wear characteristics were investigated using a pin on disc method at high temperature and speed against En-31 bearing steel disc. It was observed that …
Published in International Journal of Metallurgy and Alloys · Vol. 4, Issue 2, 2018 · pp. 1–11 Read article
-
Synthesis and Characterization of Polymer-Based Organic–Inorganic Hybrid Materials viaSol–Gel Processing: A Review of Gelatin–Silica, Gelatin–Silica–Titania and HPMA-Based Systems
Abstract: Organic–inorganic hybrid materials have emerged as a versatile class of advanced materials that integrate the flexibility and functionality of organic polymers with the thermal, mechanical, and chemical stability of inorganic networks. Among the available fabrication routes, the sol–gel process has gained considerable attention because of its simplicity, low processing temperature, compositional flexibility, and ability to tailor material properties at the molecular level. The present review discusses the synthesis and characterization …
Published in International Journal of Polymer Science and Engineering · Vol. 12, Issue 2, 2026 Read article
-
Development of an Automated Load-Controlled Thermopower Measurement Technique for Thermoelectric Materials
Abstract: The Seebeck coefficient, or thermoelectric power, is crucial. In order to deliver accurate readings over a wide temperature range, a load-based, high-precision thermoelectric power (TEP) measurement device has been designed, constructed, and experimentally validated in this study. The system is based on a differential DC approach and replaces conventional spring-based contact mechanisms with a shifting mechanical load to avoid errors caused by spring contraction, thermal cycling, and contact instability at …
Published in International Journal of Mechanics and Design · Vol. 12, Issue 1, 2026 · pp. 7–18 Read article
-
Reactivity of Niobium(V) ComplexTowards Hydroxamate Ligands
Abstract: A niobium(V) complex with the composition [NbCl(OC₆H₄CH(CH₃)₂-2)₄] was synthesized by reacting niobium pentachloride with four equivalents of 2-isopropylphenol in carbon tetrachloride as a solvent, yielding the product in good quantity. The complex was characterized using elemental analysis, molar conductance measurements, IR spectroscopy, ¹H and ¹³C NMR spectroscopy, and mass spectrometry. Spectroscopic results indicate that the complex exists in a dimeric form, with bridging occurring through isopropylphenoxo ligands. X-ray diffraction analysis …
Published in International Journal of Energetic Materials · Vol. 12, Issue 1, 2026 · pp. 1–6 Read article
-
Facile Synthesis and Electrochemical Exploration ofHexagonal Copper Sulfide (CuS) Nanocrystals for Energy Applications
Abstract: Copper sulfide (CuS) is a promising material for a variety of applications, including solar cells, lithium-ion batteries, sensors, and catalysts. In this current study, a facile technique for the synthesis of CuS nanocrystallites at modrate temperature 160°) without the use of any template or additives was reported. The reaction was carried out in a pressure reactor for 24 hours. he crystalline nature of the synthesized CuS nanocrystallites was confirmed using …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 12, Issue 1, 2026 · pp. 1–8 Read article
-
Facile Synthesis and Electrochemical Exploration ofHexagonal Copper Sulfide (CuS) Nanocrystals for EnergyApplications
Abstract: Copper sulfide (CuS) is a promising material for a variety of applications, including solar cells, lithium-ion batteries, sensors, and catalysts. In this current study, a facile technique for the synthesis of CuS nanocrystallites at modrate temperature 160°) without the use of any template or additives was reported. The reaction was carried out in a pressure reactor for 24 hours. he crystalline nature of the synthesized CuS nanocrystallites was confirmed using …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 12, Issue 1, 2026 · pp. 1–8 Read article