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65 articles for “FTIR”
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Cassia Fistula Leaf and Flower Extract and their Antibacterial Activity: A Comparative Study
Abstract: Overwhelming side effects of synthetic drugs has attracted researchers for the search and use of herbal drugs. Neem and Curcumin are very widely studied and research is still going on these species. However, Cassia Fistula, is one such plant which has various medicinal values and is less studied. Thus, the present investigation studies the extraction of leaf and flower constituents and the extract has been characterized by FTIR and NMR …
Published in International Journal of Chemical Engineering and Processing · Vol. 5, Issue 1, 2019 · pp. 1–10 Read article
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Iron Pillared Clay for Sorption of Toluene in Aqueous Solution: Kinetics and Equilibrium Studies
Abstract: The adsorption of toluene using unmodified and Fe-pillared clay were investigated in this study using UV/Visible, FT-IR spectroscopic measurements and batch adsorption process. The framework vibration of the clay before and after pillaring were determined using FTIR spectra. Effect of Contact time and initial and various concentration of toluene at constant temperature were investigated. The experimental data were studied using equilibrium isotherm (Langmuir and Freundlich) and kinetics models (pseudo first …
Published in International Journal of Chemical Engineering and Processing · Vol. 8, Issue 1, 2022 · pp. 1–10 Read article
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Pyrolysis Characteristics and Isoconversional kinetics of kusum deoiled seedcake.
Abstract: The pyrolysis characteristics and kinetics of kusum de-oiled seed cake were conducted using a Thermo gravimetric analyzer. Thermogravimetric analysis of biomass was carried out at three different heating rates of 10, 20, 30, ̊ C/min from 28 ̊ C to 1000 ̊ C under N2 atmosphere. The results indicated that the biomass was decomposed in the temperature range of 270 ̊C to 520 ̊ C and further decreased when temperature …
Published in International Journal of Environmental Chemistry · Vol. 2, Issue 2, 2016 · pp. 9–17 Read article
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Studies on Zirconium(IV) Telluroiodate: A New Heteropolyacid Based Inorganic Ion Exchange Material
Abstract: Zirconium (IV) telluroiodate has been synthesized as a new inorganic cation exchanger by adding a mixture of aqueous solution of 0.1 M potassium iodate and 0.1 M sodium tellurite to aqueous solution of 0.1 M zirconium (IV) oxychloride under varying mixing ratios at pH 1. Its ion exchange capacity for Na+ was found to be 1.85 meqg1 of dry exchanger. The material has been characterized on the basis of chemical …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 2, Issue 1, 2016 Read article
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Synthesis, characterization of Schiff base and its pH metrically studies of transition metal complexes of N'-(3, 4-dihydroxybenzylidene) isonicotinohydrazide.
Abstract: Schiff reaction is one of the versatile reaction widely used in organic synthesis focused on the discovery & development of isoniazide Schiff base derivative N’(3,4-Dihydroxy benzylidene isonicotinohydrazide) have been reported in presence of 0.01g molecular iodine catalyst stirring give fast product & good yield. The synthesized compound is characterized by FTIR & H-NMR analysis. For the development of coordination chemistry Schiff base & metal ion having played most important role, …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 6, Issue 2, 2020 · pp. 39–47 Read article
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Synthesis of Nano-ZnO by Chemical Method and its Characterization
Abstract: Nanocrystals of ZnO were prepared by chemical method using Zn (II) acetate and potassium hydroxide as the starting materials and methanol as solvent. The material was characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), electron diffraction analysis (EDS), UV-Visible spectroscopy, Dynamic light scatteringanalysis (DLS) and Fourier transform spectroscopy (FTIR) techniques. The results indicated that the obtained ZnO material was in nano-dimension and possessed pure …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 1, 2022 · pp. 13–18 Read article
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Advance in the Synthesis of Oxadiazole Based Heterocyclic Compound
Abstract: The five members of the heterocyclic ring 1,3,4-oxadiazole are necessary for the production of strong bioactive molecules. Numerous pharmacological effects, including anti-inflammatory, antibacterial, anticancer, antitubercular, anticonvulsant, anti-HIV, hypoglycemic, and antioxidant qualities, are exhibited by this intriguing class of chemicals. We have created four novel 1,3,4-oxadiazole compounds in the continuing study, which are sourced from the NSAID Ibuprofen. Melting point analysis and TLC were used to verify the compounds' purity. Open …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 2, 2023 · pp. 10–15 Read article
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Magnesium Doped Ammonium Di Hydrogen Phosphate
Abstract: New mixed crystals of Ammonium magnesium sulphate heptahydrate (AMgS) are synthesized by slow evaporation solution growth process using water as solvent. Close observation of FTIR and XRD profiles of doped and undoped samples reveal some minor structural variations. Energy dispersive spectra shows the presence of Mg (II) in the doped crystals. The sample's purity is verified through thermal analyses. SEM images exhibit defect centers due to dopants incorporation into ADP …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 40–52 Read article
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Characterization and Kinetic Study of Sugarcane Bagasse for the Production of Bio-oil Over Monodispersed Fe2 O3 and ZSM-5 Composite
Abstract: The shortage and price scramble of fossil fuels accompanied by vast CO2 emissions have triggered a worldwide search for alternative and sustainable resources. Wind, solar, geothermal, biomass, and water are the most commonly used alternative energy sources. The biomass residues are typically at low cost and readily availabile, and has been used as feedstocks for synthesis of renewable energy. To produced the bio-fuels from biomass residues, several reaction pathways categorized …
Published in International Journal of Renewable Energy and its Commercialization · Vol. 9, Issue 2, 2023 · pp. 1–13 Read article
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Preparation of Beta Lactam Compounds and Study of Thermodynamically Behavior
Abstract: Several Lactam derivatives have been prepared by condensation reaction of folic acid with (4-chloroacetophenone and 4-hydroxyacetophenone) in ethanol. Then the resultant compounds (1,2) react with another Schiff bases by reacting of 4- bromobenzaldehyde with an amino acid (Phenylalanine, Tryptophan, Tyrosine and Histidine) to give bis-β-lactam rings. The structures of target compounds were characterized by many spectroscopic methods including NMR, FTIR technique and their melting points. The β- lactam derivatives were …
Published in International journal of Thermodynamics and Chemical Kinetics · Vol. 5, Issue 2, 2019 · pp. 9–15 Read article
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Modification of Solar Hot Water Heating System
Abstract: In optoelectronics system, the copper sulfide powder plays an important role as a thin film layer. This paper covers fabrication of Copper sulfide (CuS) Powder and its characterization. The fabricated Copper sulfide powder gives better result as compared to commonly used Copper sulfide (CuS) available in the market. In this experiment, the Copper sulfide powder (CuS) was coated on the tubes as a thin film and measured the outlet water …
Published in International Journal of Water Resources Engineering · Vol. 9, Issue 1, 2023 · pp. 33–39 Read article
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Zinc oxide/Chitosan biocompatible nanocomposites: Preparation, Characterization and its use in Congo red dye photodegradation
Abstract: Zinc oxide/chitosan biocompatible nanocomposites have been successfully synthesized by co-precipitation method. The samples were characterized by X-ray diffraction (XRD), Scanning electron microscope (SEM), Energy dispersive X ray Flurescence spectroscopy (EDAX) and Fourier transformation infrared spectroscopy (FTIR). The photocatalytic efficiency and photostability of the sample was investigated systematically for Congo red degradation under solar light irradiation. UV-vis Spectroscopy was employed to investigate the optical properties and photocatalysis behavior of the Zinc …
Published in International Journal of Applied Nanotechnology · Vol. 3, Issue 2, 2017 · pp. 27–39 Read article
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To study the Properties of Bio Synthesized Silver Nanoparticles
Abstract: Recently colloids silver nanoparticles have attained much attention in global nanotechnology market due to valuable application for catalytic, biomedical, electronics and widely as Antimicrobial agents. In the present work author have synthesized and characterized the Colloids silver nanoparticles with three biosynthesis methods and the detail characterization of particle has been done by UV–Visible spectroscopy, AFM, FTIR, and with DLS techniques. Particles formation was conformed from UV spectra of nanoparticles. Size …
Published in International Journal of Applied Nanotechnology · Vol. 4, Issue 1, 2018 · pp. 34–40 Read article
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Synthesis and Characterization of Fluorescent Core-Shell Ag@SiO2 and Ag@MoS2 Nanoparticle
Abstract: Among metals, silver (Ag) and gold (Au) NPs have attracted significant interest owing to their extraordinary optical properties related with the localized surface Plasmon resonance. However, the main drawbacks of colloidal nanoparticles, making them barely useable in the photovoltaic field, are their low colloidal stability. To overcome this problem we have developed a new class of fluorescent core-shell Ag@SiO2 nanoparticles, or simply called (MEF) nanoparticles. Different characterization techniques UV-Vis, PL …
Published in International Journal of Applied Nanotechnology · Vol. 5, Issue 2, 2019 · pp. 8–16 Read article
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Execution of Poly Coatings and Corrosion of Copper
Abstract: The erosion defensive poly(aniline-co-o-toluidine) (PAOT) coatings were integrated on copper (Cu) by the electrochemical copolymerization of aniline with o-toluidine under cyclic voltammetry conditions. Fluid oxalate arrangements were utilized as the supporting electrolytes for the amalgamation of PAOT coatings on Cu. The FTIR and 1H NMR spectroscopy examines uncover that the copolymerization of aniline and o-toluidine happens on Cu substrates from a fluid oxalate arrangements and bringing about PAOT copolymer, there …
Published in International Journal of Metallurgy and Alloys · Vol. 1, Issue 2, 2015 Read article
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Bio synthesis and characterization of Gold Nanoparticles
Abstract: Colloidal Gold has attained much attention in global nanotechnology market due to valuable application in biomedical, electronics and other field as well as are being widely used as Antimicrobial agents. In this research work Gold nanoparticle suspension has been synthesized by bio synthesis method using bamboo leaves and formation of colloidal gold has been confirmed by different characterization techniques UV visible spectroscopy, FTIR and DLS. Keywords: Nanotechnology, gold Nanoparticle UV …
Published in International journal of Nanobiotechnology · Vol. 4, Issue 2, 2018 · pp. 15–20 Read article
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Formulation and Characterization of Polyhydroxyalkanoates Copolymer Nanoparticles for Controlled Drug Release
Abstract: The present study was focused on the formulation of polyhydroxyalkanoates copolymer nanoparticles (PHANPs) for in vitro controlled release of the drugs, viz. levofloxacin and amoxicillin. The PHANPs were synthesized by a triple emulsion method and conjugated with amoxicillin and levofloxacin to improve its remedial bioavailability. The PHANPs and drug conjugatedPHANPs were analysed using Scanning Electron Microscopy (SEM), Fourier Transform Infrared (FTIR) spectroscopy and X-Ray Diffraction (XRD). The cell viability % …
Published in International journal of Nanobiotechnology · Vol. 6, Issue 2, 2020 · pp. 1–11 Read article
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Synthesis and Characterization of Cesium Intercalated Graphene Thin Film
Abstract: Graphene Oxide (GO) becomes promising two-Dimensional (2D) material in optoelectronics due to its sparkling properties. In preparation step we used Carboxylation of graphene and vacuum filtration to create the free standing thin film of cesium (Cs) intercalated GO. In this work we have synthesized cesium (Cs) intercalated GO thin films at different concentration (0.03, 0.05, 0.1 mol %) by using vacuum filtration method. The functional group present in synthesized thin …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 4, Issue 1, 2018 · pp. 8–16 Read article
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Low Temperature Chemical Synthesis of Nickel Oxide Microflower and Study of its Optical and Thermal Properties
Abstract: A simple rout for the synthesis of flower like nickel oxide nanostructure has been reported using nickel sulphate and potassium per-sulphate as precursor. Efforts were made to see the effect of persulfate amount on different properties of the materials thus two samples were synthesized with different amount of per-sulphate precursors. The as prepared samples were characterized by x-ray diffraction, field emission scanning and transmission electron microscope, thermal gravimetric and differential …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 4, Issue 2, 2018 · pp. 17–24 Read article
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Preparation of Conducting Polyaniline Film for OLED Application
Abstract: Polyaniline is a conducting polymer of the semi-flexible rod polymer family, this polymer captured the intense attention of the scientific community due to the rediscovery of high electrical conductivity. In present work we have prepared the polyaniline with the chemical method and done various characterization UV – vis, FTIR, and SEM. Thin film of polyaniline is prepared with the help of spin coater and determine the I-V characteristics and also …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 5, Issue 2, 2019 · pp. 27–35 Read article