Search
104 articles for “Spectroscopic Characterization”
-
Synthesis of Nano-ZnO by Chemical Method and its Characterization
Abstract: Nanocrystals of ZnO were prepared by chemical method using Zn (II) acetate and potassium hydroxide as the starting materials and methanol as solvent. The material was characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), electron diffraction analysis (EDS), UV-Visible spectroscopy, Dynamic light scatteringanalysis (DLS) and Fourier transform spectroscopy (FTIR) techniques. The results indicated that the obtained ZnO material was in nano-dimension and possessed pure …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 8, Issue 1, 2022 · pp. 13–18 Read article
-
A Review Article: Applications of Electroanalytical Techniques
Abstract: Electroanalytical techniques are thought to be the most significant area of analytical chemistry, which identify the properties as well as quantify the given analyte(s) within an electrochemical cell. The high sensitivity, high analysis speed, low sample and solvent consumption, high scan rate, low operating cost of electro analysis make it highly advantageous in all situations. A summary of electroanalytical techniques is provided, with an emphasis on their most common uses …
Published in International Journal of Analytical and Applied Chemistry · Vol. 10, Issue 2, 2024 · pp. 13–19 Read article
-
Low temperature plasma treatment of polymeric membranes: a comparative review
Abstract: This paper presents a comparative study of plasma surface modification of various polymeric membranes. Low temperature plasma treatment using pulsed direct current discharge of different gases was employed to enhance hydrophilicity of membranes. Radio frequency discharge of various gases was used to improve surface properties of different polymeric membranes. The enhancement of hydrophilicity of the plasma modified membrane surface was evaluated by measuring the contact angle. The membranes were characterized …
Published in International Journal of Polymer Science and Engineering · Vol. 6, Issue 1, 2020 · pp. 1–19 Read article
-
Fe, Cr, Cu, Ni and Mn Concentration Determination from Matatilla Water System by Atomic Absorption Spectroscopy
Abstract: This study was conducted to assess the extent of heavy metal in the Matatilla Dam water systems. Water quality is effect by the many substance water contacts during its movement through the hydrological system. Water dissolves a wide variety of minerals, nutrients and other substance from soils, rocks and atmosphere carries them in water system. Lake streams and ground water accumulate these dissolve substance and reflect distinctive characteristic of this …
Published in International Journal of Green Chemistry · Vol. 1, Issue 2, 2015 · pp. 1–7 Read article
-
Biosynthesis, characterization of gold nanoparticles using M. indica leaf extractand their anticancer activity
Abstract: The present study involves the novel approach for the synthesis of nanomaterial holds infinite possibilities as nanotechnology has a major impact on medicine and its application. Leaf extract of Mangiferaindicais a very good bioreductant for gold chloride (HAuCl4·4H2O) which leads to the synthesis of gold nanoparticles. Leaf extract of Mangiferaindicawas mixed with gold chloride (HAuCl4·4H2O) and UV-vis spectroscopy was used to detect the synthesis of nanoparticles. TEM and FESEM were …
Published in International journal of Nanobiotechnology · Vol. 2, Issue 2, 2016 · pp. 1–4 Read article
-
Formulation and Characterization of Polyhydroxyalkanoates Copolymer Nanoparticles for Controlled Drug Release
Abstract: The present study was focused on the formulation of polyhydroxyalkanoates copolymer nanoparticles (PHANPs) for in vitro controlled release of the drugs, viz. levofloxacin and amoxicillin. The PHANPs were synthesized by a triple emulsion method and conjugated with amoxicillin and levofloxacin to improve its remedial bioavailability. The PHANPs and drug conjugatedPHANPs were analysed using Scanning Electron Microscopy (SEM), Fourier Transform Infrared (FTIR) spectroscopy and X-Ray Diffraction (XRD). The cell viability % …
Published in International journal of Nanobiotechnology · Vol. 6, Issue 2, 2020 · pp. 1–11 Read article
-
Protein Determination and Soluble Amino Acids Prediction in Various Solvents Extracted Solutions of Indigenous Red Lentil and Moong Pulse through Direct UV- Visible Spectrophotometer Technique: A Comparative Study
Abstract: In this comparative study, direct protein determination have been done for indigenous Red lentil (Lens culinaris) and Moong pulse (Vigna radiata) (obtained from Muzaffarpur, Bihar) by UV-Visible spectroscopy in three different solvents viz. double distilled water (ddH2O), ethyl alcohol (C2H5OH), and methyl alcohol (CH3OH). A few amino acids in solutions have also been predicted (not characterized) based on their peaks observed in UV-region by comparing them with reported range of …
Published in International Journal of Plant Biotechnology · Vol. 9, Issue 2, 2023 · pp. 42–48 Read article
-
Commercial Scale Quantification of Lignin
Abstract: Lignin, an aromatic biopolymer, in the terrestrial lignocellulosic biomass constitutes the single largest and sustainable source of biofuels and biochemicals. The recalcitrant nature of lignin is a hindrance to its chemical or biochemical conversion. Moreover, its insolubility in water too is a major challenge in its quantification which is a necessary step prior to and after its conversion. Though there are celebrated quantification methods like the classical Klason lignin method …
Published in International Journal of Environmental Chemistry · Vol. 11, Issue 2, 2025 · pp. 20–25 Read article
-
Electrodeposition of Bright Zn–Co–Fe Alloy Coatings on Mild Steel and Their Characterization
Abstract: Sulphate bath having ZnSO4. 7H2O, CoSO4. 7H2O, FeSO4.7H2O and thiamine hydrochloride (THC) and citric acid (CA) in combination, was optimized for deposition of bright Zn–Co–Fe alloy coating on mild steel. Bath constituents and operating parameters were optimized by Hull cell method, for highest corrosion performance against coating. The effect of current density on deposit characters viz., corrosion resistance, hardness, thickness, CCE were evaluated. Potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) …
Published in International Journal of Analytical and Applied Chemistry · Vol. 2, Issue 2, 2016 · pp. 17–25 Read article
-
Green Synthesis of Silver Nanoparticles from Trapa bispinosa Fruit Extract: Characterization and Promising Antimicrobial Activity Against Multidrug-Resistant Pathogens
Abstract: Silver nanoparticles (Ag NPs) are widely recognized for their applications in medicine, electronics, and environmental remediation. This study presents a new green synthesis method for Ag NPs using Trapa bispinosa fruit extract as a natural reducing agent and stabilizing agent. Characterization of the synthesized Ag NPs through X-ray diffraction (XRD) confirmed a crystalline structure consistent with the face-centered cubic (fcc) arrangement, with peaks at (111), (200), (220), (311), and (222), …
Published in International Journal of Applied Nanotechnology · Vol. 11, Issue 1, 2025 · pp. 38–46 Read article
-
Bioethanol Production from Corncob Cellulosic Biomass: RSM and ANN based Optimization for Dilute Acid Pretreatment
Abstract: To increase the yield of fermentable sugars, the complexity of lignocellulosic biomass requires a pretreatment method. Dilute acid hydrolysis was used to efficiently pretreatment corn cobs. The aim of this study was to characterize corncob and investigate the effect of process parameters on total reducing sugar (TRS) yield during dilute acid hydrolysis pretreatment of corncob biomass. The morphology and microstructure of the samples were examined using an X-ray diffraction machine, …
Published in International Journal of Chemical Engineering and Processing · Vol. 9, Issue 2, 2023 · pp. 16–34 Read article
-
Larvicidal Activities of Biosynthesized Zinc and Nickel Nanoparticles using Allium sativum (Garlic) oil on Anopheles spp Larvae Yobe State, Nigeria
Abstract: Emergence of insecticide resistance and their harmful effects on non-target organisms and environment has necessitated an urgent search for development of new and improved mosquito control methods that are effective and safe for non-target organisms and the environment. The present study aims to assess the larvicidal activities of biosynthesized zinc and Nickel Nanoparticles using Allium sativum (garlic) oil against the larvae of malaria Anopheles spp. The garlic oil extracted was …
Published in International journal of Nanobiotechnology · Vol. 7, Issue 2, 2021 · pp. 1–9 Read article
-
Influence of CeO2 nanoparticles on the corrosion behavior of electrodeposited Ni coatings
Abstract: Nickel-Ceria (Ni-CeO2) nanocomposite coatings were developed on mild steel (MS) substrate using electrodeposition method. The codeposition of the nanoparticles was achieved from the optimized Ni plating bath loaded with CeO2 nanoparticles (particle size <20 nm). Ni and Ni-CeO2 coatings were achieved at a wide current density (c.d.) range from 1.0 to 5.0 A/dm2 under optimal conditions, and their corrosion protection efficacy was examined in 5% NaCl medium. The material property …
Published in International Journal of Chemical Engineering and Processing · Vol. 2, Issue 1, 2016 · pp. 19–28 Read article
-
Synthesis, Crystal Growth and Characterization of Bismuth Doped Potassium Hydrogen Phthalate Crystal (Khp): A Nlo Material
Abstract: To create single crystals using the Slow Evaporation Solution Growth Technique (SEST), equimolar composition of the transition metal (Bi) as Bismuth nitrate is added to Potassium Hydrogen Phthalate (KHP) (1:1) at ambient temperature. The following analysis is then performed on the single crystals that have formed. Equimolar doping-induced structural distortion in the crystals is confirmed by the FT-IR Spectra. The TGDTA study reveals the purity of the material and no …
Published in International Journal of Composite Materials and Matrices · Vol. 10, Issue 1, 2024 · pp. 19–27 Read article
-
Synthesis, Characterization, Antibacterial Study and Study of Bio Properties for New Analytical Reagents
Abstract: Due to the widespread pollution of heavy metals in water and environmental samples, the pollution levels have increased. Therefore, researchers have begun working on various environmental solutions to improve the levels of these elements in environmental samples. One such solution is the preparation of analytical reagents as coordination agents and ligands to shield the elements from water and soil, thereby reducing pollution levels. In this study, new analytical reagents were …
Published in International Journal of Environmental Chemistry · Vol. 12, Issue 1, 2026 · pp. 1–11 Read article
-
Cognitive Metallurgy: A Study on Microstructure and Energy Efficiency in High-Temperature Alloying via Sensor Fusion and Deep Reinforcement Learning
Abstract: Background Traditional high-temperature metallurgical processes, such as continuous casting and specialty alloy synthesis, are characterized by high energy consumption, stochastic variability, and reliance on post-process defect inspection. The inability to precisely monitor, model, and predict the real-time thermal, chemical, and mechanical state of molten metal and cooling substrates results in significant material waste and inconsistent microstructural integrity. Methodology This study introduces a novel framework for Cognitive Metallurgy utilizing an integrated …
Published in International Journal of Metallurgy and Alloys · Vol. 11, Issue 2, 2025 · pp. 27–36 Read article
-
Experimental Study on Charging Conditions of a Single Component DDT Detonator Using Nickel Hydrazine Nitrate
Abstract: As a salt of a coordination compound of nickel, nickel hydrazine nitrate (NHN) is an energetic substance with characteristics halfway between those of primary and secondary explosives. It is less sensitive to friction and mechanical impact than other primary explosives, although it is highly sensitive to flames. NHN is not very dangerous to handle, but it explodes readily when exposed to flame. This property makes it possible to fabricate safety …
Published in International Journal of Energetic Materials · Vol. 11, Issue 2, 2025 · pp. 1–12 Read article
-
Induced codeposition of Ni-W alloy coatings using glycerol as additive and their characterization
Abstract: As a promising coating material to replace hard chromium coating, the development of nickel–tungsten (Ni-W) alloy coatings of good corrosion protection is of great interest in surface coating technology. Further, the effect of plating variables, including additive on the composition of alloys of induced co-deposition is more vagarious than in other types of alloy deposition. In this regard, an alkaline citrate bath has been formulated for electrodeposition of Ni-W alloy …
Published in International Journal of Chemical Engineering and Processing · Vol. 2, Issue 2, 2016 · pp. 1–9 Read article
-
Mechanical and Microstructure Properties of Al and SiC Reinforced Aluminum-Based Metal Matrix Composite
Abstract: It is becoming increasingly difficult to design new technical materials that are resistant to wear damage and corrosion degradation in severe service circumstances. Unfortunately, even with crucial passive metals, like Al alloys, there is often a compromise between wear and corrosion resistance. Because of the unfavorable galvanic connection between the precipitates and the matrix, precipitates not only harden the material but also accelerate corrosion. This research established that a supersaturated …
Published in International Journal of Metallurgy and Alloys · Vol. 11, Issue 1, 2025 · pp. 26–43 Read article
-
Modification of Solar Hot Water Heating System
Abstract: In optoelectronics system, the copper sulfide powder plays an important role as a thin film layer. This paper covers fabrication of Copper sulfide (CuS) Powder and its characterization. The fabricated Copper sulfide powder gives better result as compared to commonly used Copper sulfide (CuS) available in the market. In this experiment, the Copper sulfide powder (CuS) was coated on the tubes as a thin film and measured the outlet water …
Published in International Journal of Water Resources Engineering · Vol. 9, Issue 1, 2023 · pp. 33–39 Read article