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61 articles for “x-ray microscope”
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Low Temperature Chemical Synthesis of Nickel Oxide Microflower and Study of its Optical and Thermal Properties
Abstract: A simple rout for the synthesis of flower like nickel oxide nanostructure has been reported using nickel sulphate and potassium per-sulphate as precursor. Efforts were made to see the effect of persulfate amount on different properties of the materials thus two samples were synthesized with different amount of per-sulphate precursors. The as prepared samples were characterized by x-ray diffraction, field emission scanning and transmission electron microscope, thermal gravimetric and differential …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 4, Issue 2, 2018 · pp. 17–24 Read article
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Tailoring Electrolytic Deposition of Zn-Ni Alloys for Superior Corrosion Resistance in Harsh Environments
Abstract: Since Zn–Ni alloy coatings are more resistant to corrosion than pure zinc coatings, they are being researched extensively. In this study, Zn–Ni alloy coatings electrolytically deposited from an acidic sulfate bath are investigated. The study looks into how the microstructure, phase composition, and corrosion resistance of the coatings are affected by deposition factors like pH, current density, and electrolyte composition. X-ray diffraction (XRD), potentiodynamic polarization, and scanning electron microscopy (SEM) …
Published in International Journal of Chemical Engineering and Processing · Vol. 11, Issue 1, 2025 Read article
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Induced codeposition of Ni-W alloy coatings using glycerol as additive and their characterization
Abstract: As a promising coating material to replace hard chromium coating, the development of nickel–tungsten (Ni-W) alloy coatings of good corrosion protection is of great interest in surface coating technology. Further, the effect of plating variables, including additive on the composition of alloys of induced co-deposition is more vagarious than in other types of alloy deposition. In this regard, an alkaline citrate bath has been formulated for electrodeposition of Ni-W alloy …
Published in International Journal of Chemical Engineering and Processing · Vol. 2, Issue 2, 2016 · pp. 1–9 Read article
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Nanostructured Carbon Aloe vera based DSSC Solar Cell Using Screen Printing Technology
Abstract: Today every nation faces vitality emergencies; so, to conquer it, various arrangements are given to advance towards sun-based energy harvesting which is rich and allowed to utilize. The presented study aims to give a simple synthesis technique for mass production of DSSC from working principles to the first commercial use. DSSC converts solar energy into electricity with help of energy harvesting materials like natural dye which makes it more sustainable …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 6, Issue 2, 2020 · pp. 52–59 Read article
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Sorption of Pb (II), Cd(II) and Zn(II) by synthesized nanocrystalline sodium potassium flurophlogopite (FGP)
Abstract: We have successfully synthesized nanocrystalline sodium potassium fluorophlogopite (FGP) crystals with controlled sizes from ≈ 25 nm to 100nm, using an organic tetrapropylammonium (TPA) hydroxide. We have been successfully synthesized material depends on the source of silicate and hydrothermal crystallization conditions. The synthesized materials were characterized by using different techniques such as X-ray diffraction, Energy Dispersive Analysis, Scanning Electron Microscope, Transmission Electron Microscopy and FTIR analysis. The use of sodium …
Published in International Journal of Composite Materials and Matrices · Vol. 9, Issue 2, 2023 · pp. 41–49 Read article
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Pyrolysis Characteristics and Isoconversional kinetics of kusum deoiled seedcake.
Abstract: The pyrolysis characteristics and kinetics of kusum de-oiled seed cake were conducted using a Thermo gravimetric analyzer. Thermogravimetric analysis of biomass was carried out at three different heating rates of 10, 20, 30, ̊ C/min from 28 ̊ C to 1000 ̊ C under N2 atmosphere. The results indicated that the biomass was decomposed in the temperature range of 270 ̊C to 520 ̊ C and further decreased when temperature …
Published in International Journal of Environmental Chemistry · Vol. 2, Issue 2, 2016 · pp. 9–17 Read article
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Formulation and Characterization of Polyhydroxyalkanoates Copolymer Nanoparticles for Controlled Drug Release
Abstract: The present study was focused on the formulation of polyhydroxyalkanoates copolymer nanoparticles (PHANPs) for in vitro controlled release of the drugs, viz. levofloxacin and amoxicillin. The PHANPs were synthesized by a triple emulsion method and conjugated with amoxicillin and levofloxacin to improve its remedial bioavailability. The PHANPs and drug conjugatedPHANPs were analysed using Scanning Electron Microscopy (SEM), Fourier Transform Infrared (FTIR) spectroscopy and X-Ray Diffraction (XRD). The cell viability % …
Published in International journal of Nanobiotechnology · Vol. 6, Issue 2, 2020 · pp. 1–11 Read article
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Characterization of CeO2-NiO Thin Film Produced by Jet Nebuliser Technique
Abstract: CeO2 –NiO composite solution was sprayed as thin films by using JET nebulizer technique at the substrate temperature of 250°C. The film was characterized by X-ray diffractometer and crystallite size, lattice constant, crystallinities, phase transformations were measured. The UV-Vis spectrometer analysis was used to calculate the band gap, absorbance and percentage of transmission of the thin films was reported. The emission and excitation spectra of the sample were reported. The …
Published in International journal of Nanobiotechnology · Vol. 7, Issue 1, 2021 · pp. 1–17 Read article
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Synthesis, characterization, antibacterial activity and in-vitro cytotoxicity of Dy and Fe doped hydroxyapatite nanomaterials
Abstract: Dy- and Fe-doped hydroxyapatite (HAp) was synthesized by the facile aqueous precipitation method. The samples were characterized by using powder X-ray diffraction, Fourier transform infrared spectroscopy and transmission electron microscopy. In this work, the antibacterial activities of Dy- and Fe-doped HAp were tested against gram-positive (Staphylococcus aureus, Bacillus subtilis) and gram-negative (Escherichia coli, Klebsiella pneumoniae and Pseudomonas putida) bacteria by agar diffusion test. It was found that Dy(5)-and Fe(5)-doped HAp …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 4, Issue 1, 2018 · pp. 46–54 Read article
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Design and Analysis of Metal-Organic Frameworks for Gas Adsorption and Storage
Abstract: Metal-Organic Frameworks (MOFs) represent a class of highly porous materials formed by the coordination of metal ions with organic linkers, exhibiting exceptional potential for gas storage applications due to their high surface area, tunable pore sizes, and structural versatility. The synthesis and characterization of MOFs intended for the effective storage of gases like carbon dioxide, methane, and hydrogen are the main topics of this work. Solvothermal Hectic strategies, including solvothermal, …
Published in International Journal of Metallurgy and Alloys · Vol. 10, Issue 1, 2024 · pp. 25–30 Read article
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Investigation of the Optical-Electrical Properties of Simonkolleite and ZnO: Synergism and Nano/Microcrystals
Abstract: This study aimed to investigate the optical-electrical properties of simonkolleite (SM) and zinc oxide (ZnO), focusing on ZnO's nano/micro size and the synergistic effects between SM and ZnO. The synthesis of SM nanocrystals (NCs) was successfully achieved, and thermal annealing temperature was used to manipulate the formation of SM/ZnO nanocomposites ranging from NCs to microcrystals of ZnO. Structural and morphological properties were characterized using X-ray diffraction (XRD),Fourier transforms infrared (FT-IR), …
Published in International Journal of Energetic Materials · Vol. 8, Issue 2, 2022 · pp. 18–30 Read article
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Synthesis, Spectral Study, SEM Analysis and Antibacterial Study of New Indole Azo Ligand and Complexes
Abstract: Azo ligands have developed significantly in recent decades due to their fundamental role in the coordination chemistry of transition elements. Their rapid response to coordination bonding in ligand and complex chemistry, particularly with divalent ions, is a key factor. The azo-bridged bond has played a well-established role in the formation of cobalt, nickel, and copper complexes. In this study, we prepared a novel ligand, an indole derivative bonded to an …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 12, Issue 1, 2026 · pp. 1–10 Read article
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Comparative study of the Magnetoelectric Properties in Core-Shell Nanocomposites as well as mixture of CoFe2O4:BaTiO3
Abstract: Nanostructures of multiferroic materials have been drawing increasing curiosity due to the boosted magnetoelectric coupling and potential for succeeding generation multifunctional devices. Composites of ferroelectric and magnetostrictive materials indicate more magnetoelectric coupling than single phase materials. Core-shell CoFe2O4:BaTiO3 nanocomposites (1:1 weight ratio) and a mixture of both of them have been produced by a combination of hydrothermal and sol gel techniques. X ray diffraction analysis endorses the presence of both …
Published in International Journal of Composite and Constituent Materials · Vol. 1, Issue 1, 2015 · pp. 1–6 Read article
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Synthesis and characterization of high saline water resistant sulphur composite from petrochemical waste
Abstract: Petrochemical industry produces variety of side products and waste materials like sulphur, spent catalysts, spent adsorbents, etc. These waste materials can be converted to the value-added products by forming their composites with unique properties. For example, sulphur due to its chemical properties like high resistivity to corrosive environment, hydrophobic nature, antifungal property, its composite can be prepared and used in construction industries as a substitute for cement composite material. To …
Published in International Journal of Green Chemistry · Vol. 6, Issue 2, 2020 · pp. 64–77 Read article
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Investigation on Synthesis and Evaluation of Nanopore NaA Zeolite Membranes
Abstract: Effects of synthesis parameters on the membrane structure and performance have been investigated for nanopore NaA zeolite membranes grown onto seeded mullite supports. Molar composition of the starting gel of nano NaA membranes was: SiO2/Al2O3=0.8–3.2, Na2O/Al2O3=1.6–4.6, and H2O/Al2O3=50–200. Also, effects of crystallization time and temperature on the membrane performance were studied. X-ray diffraction (XRD) patterns of the membranes exhibited peaks corresponding to the support and the zeolite. The crystal species …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 2, 2017 · pp. 9–22 Read article
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Preparation and Evaluation of Nano pore Faujasite Membranes
Abstract: Nano pore Faujasite zeolite membranes were synthesized by in-situ hydrothermal method on porous ceramic tubes. Hydrothermal crystallization was carried out under an autogenously pressure and at a static condition of 100 oC. Molar composition of the starting gel of Faujasite zeolite membranes were NaX: SiO2/Al2O3=10-27, Na2O/Al2O3=4-9, H2O/Al2O3=250; NaY: SiO2/Al2O3=2.5-4, Na2O/SiO2=1.08-2, H2O/Na2O=30-200. X-ray diffraction (XRD) patterns of the membranes exhibited peaks corresponding to the support and the zeolite. The crystal species …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 3, Issue 2, 2017 · pp. 15–24 Read article
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Study of Dynamic Mechanical and Thermal Properties of Poly(Ether Ether Ketone) Carbon Nanotubes
Abstract: The effect of polyetherimide (PEI) as a compatibilizing agent on the morphology, thermal, electrical and dynamic-mechanical properties of poly(ether ether ketone) (PEEK)/single-walled carbon nanotube (SWCNT) nanocomposites, has been investigated for different CNT loadings. After a pre-processing step based on ball milling and premixing under mechanical treatments in ethanol, the samples were prepared by melt extrusion. A more homogeneous distribution of the CNTs throughout the matrix is found for composites containing …
Published in International Journal of Polymer Science and Engineering · Vol. 3, Issue 1, 2017 · pp. 1–21 Read article
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Facile Synthesis and Electrochemical Exploration ofHexagonal Copper Sulfide (CuS) Nanocrystals for Energy Applications
Abstract: Copper sulfide (CuS) is a promising material for a variety of applications, including solar cells, lithium-ion batteries, sensors, and catalysts. In this current study, a facile technique for the synthesis of CuS nanocrystallites at modrate temperature 160°) without the use of any template or additives was reported. The reaction was carried out in a pressure reactor for 24 hours. he crystalline nature of the synthesized CuS nanocrystallites was confirmed using …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 12, Issue 1, 2026 · pp. 1–8 Read article
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Facile Synthesis and Electrochemical Exploration ofHexagonal Copper Sulfide (CuS) Nanocrystals for EnergyApplications
Abstract: Copper sulfide (CuS) is a promising material for a variety of applications, including solar cells, lithium-ion batteries, sensors, and catalysts. In this current study, a facile technique for the synthesis of CuS nanocrystallites at modrate temperature 160°) without the use of any template or additives was reported. The reaction was carried out in a pressure reactor for 24 hours. he crystalline nature of the synthesized CuS nanocrystallites was confirmed using …
Published in International Journal of Nanomaterials and Nanostructures · Vol. 12, Issue 1, 2026 · pp. 1–8 Read article
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Green Synthesis of Silver Nanoparticles from Trapa bispinosa Fruit Extract: Characterization and Promising Antimicrobial Activity Against Multidrug-Resistant Pathogens
Abstract: Silver nanoparticles (Ag NPs) are widely recognized for their applications in medicine, electronics, and environmental remediation. This study presents a new green synthesis method for Ag NPs using Trapa bispinosa fruit extract as a natural reducing agent and stabilizing agent. Characterization of the synthesized Ag NPs through X-ray diffraction (XRD) confirmed a crystalline structure consistent with the face-centered cubic (fcc) arrangement, with peaks at (111), (200), (220), (311), and (222), …
Published in International Journal of Applied Nanotechnology · Vol. 11, Issue 1, 2025 · pp. 38–46 Read article