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84 articles for “Scanning Electron Microscopy”
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Magneto-electrodeposition of Sn–Ni alloy Coating for Better Corrosion Protection
Abstract: The present paper reports the development of excellent corrosion resistant Sn–Ni alloy coatings from a new pyrophosphate bath by magneto-electrodeposition (MED) approach. First part reports optimization of conditions for deposition of Sn–Ni coatings on mild steel by conventional electrodeposition (ED) method and their characterization. The second part demonstrates how the corrosion resistance of Sn–Ni alloy coatings can be improved drastically by MED method, using same bath. Significant decrease of corrosion …
Published in International Journal of Chemical Engineering and Processing · Vol. 2, Issue 1, 2016 · pp. 29–42 Read article
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Induced codeposition of Ni-W alloy coatings using glycerol as additive and their characterization
Abstract: As a promising coating material to replace hard chromium coating, the development of nickel–tungsten (Ni-W) alloy coatings of good corrosion protection is of great interest in surface coating technology. Further, the effect of plating variables, including additive on the composition of alloys of induced co-deposition is more vagarious than in other types of alloy deposition. In this regard, an alkaline citrate bath has been formulated for electrodeposition of Ni-W alloy …
Published in International Journal of Chemical Engineering and Processing · Vol. 2, Issue 2, 2016 · pp. 1–9 Read article
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Electrolytic Deposition of Zn–Ni Alloy from Acidic Sulphate Bath and Their Characterization
Abstract: A bath containing ZnSO4.7H2O, NiSO4.7H2O, thiamine hydrochloride (THC) and citric acid (CA) has been proposed. Bright Zn–Ni alloy coatings were developed galvanostatically onto mild steel (MS) and their corrosion resistance and other physical properties were studied. THC was found to improve the brightness and homogeneity of the deposit. The dependency of bath composition, current density (c.d.), pH and temperature, agitation on wt.% Ni were tested. Deposition was carried out under …
Published in International Journal of Chemical Engineering and Processing · Vol. 2, Issue 2, 2016 · pp. 19–32 Read article
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Production of Compositionally Modulated Nanolayer Zn–Ni Alloy Coatings and Their Corrosion Behaviours
Abstract: Compositionally modulated nanolayer alloy (CNA) coatings of Zn–Ni having alternatively the same compositions have been developed galvanostatically on mild steel from single bath technique (SBT) using square current pulses. Sulphanilic acid and citric acid (CA) were used as additives. Modulation in the composition of alloys were introduced by passing a different switched cathode current densities (SCCD’S) using sophisticated power sources. Variety of CNA coatings was developed under different conditions of …
Published in International Journal of Chemical Engineering and Processing · Vol. 3, Issue 1, 2017 · pp. 1–8 Read article
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Chemical Synthesis and Characterization of Polyaniline for Supercapacitors Application
Abstract: Various polyaniline (PANI) synthesis methods are reported in the literature, depending on the experimental parameters involved (T, t, doping, and mixing procedure). Herein, three chemical polymerization methods were used to synthesis PANI from aniline monomer: rapid oxidation (OR), controlled oxidation (CO), and interfacial oxidation (OI). The PANI was therefore deposited next by drop casting on a silicon (Si) substrate. X-ray diffraction, Raman spectroscopy, and scanning electron microscopy were used to …
Published in International Journal of Chemical Engineering and Processing · Vol. 8, Issue 2, 2022 · pp. 9–16 Read article
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Pyrolysis Characteristics and Isoconversional kinetics of kusum deoiled seedcake.
Abstract: The pyrolysis characteristics and kinetics of kusum de-oiled seed cake were conducted using a Thermo gravimetric analyzer. Thermogravimetric analysis of biomass was carried out at three different heating rates of 10, 20, 30, ̊ C/min from 28 ̊ C to 1000 ̊ C under N2 atmosphere. The results indicated that the biomass was decomposed in the temperature range of 270 ̊C to 520 ̊ C and further decreased when temperature …
Published in International Journal of Environmental Chemistry · Vol. 2, Issue 2, 2016 · pp. 9–17 Read article
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Effect of TiO2 on HER Activity of Electrodeposited Zn–Ni Coatings
Abstract: This paper demonstrates the improved electrocatalytic behavior of Zn–Ni alloy coatings for alkaline hydrogen evolution reaction (HER), due to addition of TiO2 nanoparticles into the bath. Zn–Ni alloy coatings have been electrodeposited galvanostatically on copper, with wide compositional range (2.31–7.91 wt. % of Zn) at different current densities (c.d.) between 2.0 and 5.0 A dm-2. The electrocatalytic behaviors of all coatings have been studied for alkaline HER in 1.0 M …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 3, Issue 1, 2017 Read article
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Preparation and Evaluation of Nano pore Faujasite Membranes
Abstract: Nano pore Faujasite zeolite membranes were synthesized by in-situ hydrothermal method on porous ceramic tubes. Hydrothermal crystallization was carried out under an autogenously pressure and at a static condition of 100 oC. Molar composition of the starting gel of Faujasite zeolite membranes were NaX: SiO2/Al2O3=10-27, Na2O/Al2O3=4-9, H2O/Al2O3=250; NaY: SiO2/Al2O3=2.5-4, Na2O/SiO2=1.08-2, H2O/Na2O=30-200. X-ray diffraction (XRD) patterns of the membranes exhibited peaks corresponding to the support and the zeolite. The crystal species …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 3, Issue 2, 2017 · pp. 15–24 Read article
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Green Chemistry Approach for the Preparation of Silver Nanoparticles: A Review
Abstract: The word "nanoparticles" refers to particles within a size range of 10 and 100 nm. Nanotechnology is the topic that is growing the fastest because of its applications in science and technology to produce new at the nanoscale range. Silver is the metal of first preference among the various noble metals. The production of silver nanoparticles can be achieved by different methods such as: chemical method, biological method, green synthesis. …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 30–39 Read article
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Synthesis, Crystal growth and Characterization of Lead acetate zinc (II)Sulphate Material
Abstract: Leadacetatezinc (II) Sulphate Crystal is synthesized by the addition of Leadacetate to Zinc sulphate in equimolar concentration (1:1ratio) to produce larger sized crystal but during the crystallization process a bulk of colourless precipitate was obtained and after filtration the crystals are formed in the filtrate after slow evaporation solution growth technique. Thus formed crystals from the filtrate is kept away and the precipitate formed during the crystallization process is characterized …
Published in International Journal of Chemical Synthesis and Chemical Reactions · Vol. 9, Issue 1, 2023 · pp. 22–29 Read article
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Synthesis and Characterization of Magnetite-Pectin-Alginate Hybrid and Bionanocomposite
Abstract: It is a one pot synthesis of hybrid bionanocomposite comprising of inorganic magnetite with stabilizer biopolymer pectin and alginate in co-precipitation method using sodium hydroxide and ammonium hydroxide as precipitating agents. A lot of comparison and investigation has been done in particle size of nanocomposite by changing the stoichiometric ratio of both magnetite and biopolymer concentration and drying condition of composite. The nanocomposite has been characterized using infrared spectroscopy (FTIR), …
Published in International Journal of Applied Nanotechnology · Vol. 3, Issue 1, 2017 · pp. 18–22 Read article
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Investigation of the Optical-Electrical Properties of Simonkolleite and ZnO: Synergism and Nano/Microcrystals
Abstract: This study aimed to investigate the optical-electrical properties of simonkolleite (SM) and zinc oxide (ZnO), focusing on ZnO's nano/micro size and the synergistic effects between SM and ZnO. The synthesis of SM nanocrystals (NCs) was successfully achieved, and thermal annealing temperature was used to manipulate the formation of SM/ZnO nanocomposites ranging from NCs to microcrystals of ZnO. Structural and morphological properties were characterized using X-ray diffraction (XRD),Fourier transforms infrared (FT-IR), …
Published in International Journal of Energetic Materials · Vol. 8, Issue 2, 2022 · pp. 18–30 Read article
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Effect of Ge and Pb Impurities on the Optical Properties of Amorphous (Sb2Se3)90Sn10 Thin Films
Abstract: The as prepared samples of [(Sb2Se3)90Sn10]95 M5 [M = Ge, Pb] chalcogenide system were amorphous as evidenced by X-ray diffraction studies. The optical band gap has been estimated with the help of Taucs relation for the as-deposited [(Sb2Se3)90Sn10]95M5 thin films. It is observed that the optical band gap increase with increase in the Ge and Pb content, which may be due to decrease in the density of defect states. This …
Published in International Journal of Metallurgy and Alloys · Vol. 6, Issue 1, 2020 · pp. 7–14 Read article
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Modern Material Concept to Produce Low-Loss Non- Oriented Electric Alloys
Abstract: The production of energy-efficient materials is an essential aspect of modern society, with efforts focused on reducing energy loss and conserving resources. A key element in the creation of energy-efficient electrical equipment, such as transformers, generators, and motors, is low-loss non-oriented electrical steel. In this regard, material design is a promising approach to improve the properties of non-oriented electrical steel. This paper presents an overview of material design for low-loss …
Published in International Journal of Metallurgy and Alloys · Vol. 8, Issue 2, 2022 · pp. 37–42 Read article
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Biosynthesis of Chitosan mediated nanoparticles for Preservation of Food and Its Antimicrobial activity
Abstract: In this study, chitosan nanoparticles were synthesized from chitosan polymer by ionic gelation method. The chitin was first extracted from Saccharomyces cerevisiae and then deacetylated to chitosan. The presence and characterization of chitosan nanoparticles was investigated by UV-Visible Spectroscopy (UV) and scanning electron microscopy (SEM). The antimicrobial property of these chitosan nanoparticles were studied against E.coli, S.aureus, S.typhi, P.aureginosa, C.albicans and A.niger and compare with chitosan polymer. CSNPs showed higher …
Published in International journal of Nanobiotechnology · Vol. 3, Issue 1, 2017 · pp. 16–24 Read article
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Synthesis of chitosan mediated nanoparticles and its antimicrobial activity
Abstract: In this study, chitosan nanoparticles were synthesized from chitosan polymer by ionic gelation method. The chitin was first extracted from crab shell and then deacetylated to chitosan. The presence and characterization of chitosan nanoparticles was investigated by UV-Visible Spectroscopy (UV) and scanning electron microscopy (SEM). The antimicrobial property of these chitosan nanoparticles were studied against E.coli, S.aureus, S.typhi, P.aureginosa, C.albicans and A.niger and compare with chitosan polymer. CSNPs showed higher …
Published in International journal of Nanobiotechnology · Vol. 3, Issue 2, 2017 · pp. 31–35 Read article
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Biosynthesis of silver nanoparticles using aqueous leaf extract of Muntingia calabura Linn.
Abstract: The present study was focused to synthesis silver nanoparticles using the aqueous leaf extract of Muntingia calabura L. as the reducing agent. The formation of silver nanoparticles was confirmed by colour change from light yellow to dark brownish red, UV-Visible Spectroscopy, FT-IR, X-Ray Diffraction Method (XRD), Scanning Electron Microscopy (SEM) and Energy Dispersive X-ray microanalysis spectroscopy (EDS). The nanoparticles showed an absorbance at 443nm on UV-Visible spectroscopy. The presence of …
Published in International journal of Nanobiotechnology · Vol. 4, Issue 1, 2018 · pp. 9–15 Read article
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Formulation and Characterization of Polyhydroxyalkanoates Copolymer Nanoparticles for Controlled Drug Release
Abstract: The present study was focused on the formulation of polyhydroxyalkanoates copolymer nanoparticles (PHANPs) for in vitro controlled release of the drugs, viz. levofloxacin and amoxicillin. The PHANPs were synthesized by a triple emulsion method and conjugated with amoxicillin and levofloxacin to improve its remedial bioavailability. The PHANPs and drug conjugatedPHANPs were analysed using Scanning Electron Microscopy (SEM), Fourier Transform Infrared (FTIR) spectroscopy and X-Ray Diffraction (XRD). The cell viability % …
Published in International journal of Nanobiotechnology · Vol. 6, Issue 2, 2020 · pp. 1–11 Read article
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Characterization of CeO2-NiO Thin Film Produced by Jet Nebuliser Technique
Abstract: CeO2 –NiO composite solution was sprayed as thin films by using JET nebulizer technique at the substrate temperature of 250°C. The film was characterized by X-ray diffractometer and crystallite size, lattice constant, crystallinities, phase transformations were measured. The UV-Vis spectrometer analysis was used to calculate the band gap, absorbance and percentage of transmission of the thin films was reported. The emission and excitation spectra of the sample were reported. The …
Published in International journal of Nanobiotechnology · Vol. 7, Issue 1, 2021 · pp. 1–17 Read article
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Trichoderma Based Synthesis of Silver Oxide Nanoparticles, Their Characterization and Assessment of Antifungal Activity
Abstract: The fungal spore suspension of Trichoderma harzianum was used for the preparation of AgO nanoparticles. T. harzianum spore suspension acts as reducing and stabilizing agent for the fabrication of nanoparticles. The synthesized nanoparticles were characterized by X-ray diffractometry (XRD), scanning electron microscopy (SEM), energy dispersive X-analysis (EDAX) and transmission electron microscopy (TEM). The AgO nanoparticles were circular in shape with average diameter 10-20 nm. The AgO nanoparticles showed promising antifungal …
Published in International journal of Nanobiotechnology · Vol. 7, Issue 2, 2021 · pp. 19–25 Read article