International Journal of Analytical and Applied Chemistry
Volume 3, Issue 1 (2017)
Published
Table of contents
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A New Spectrophotometric Method for the Determination of Psilocin and Psilocybin
Abstract: A rapid new spectrophotometric method is developed for the determination of psilocin and psilocybin using the oxidative coupling reaction with 3-methylbenzthiazolinone-2-hydrazone. The method is precise and accurate. It can be applied to the estimation of psilocin and psilocybin in forensic exhibits. Keywords: 3-methylbenzthiazolinone-2-hydrazone, psilocin, psilocybin, spectrophotometry
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 1, 2017 · pp. 1–8 Read article
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Spectrophotometric Determination of Salicylates in Urine using 3-Methylbenzthiazolinone – 2 – hydrazone
Abstract: A sensitive (direct or with column partition chromatography) spectrophotometric method for the determination of salicylates in urine using 3 – methylbenzthiazolinone - 2 – hydrazone in the presence of ceric ammonium sulfate as an oxidizing agent is presented. Beer’s law is obeyed in the concentration range of 0 – 1.6 µg ml -1. The method is accurately reproducible and can be applied in the analysis of salicylates in urine. The …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 1, 2017 · pp. 14–17 Read article
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Functionalization of Reclaim Rubber: Possible Precursor for Polyblends in Engineering Applications
Abstract: Improvements in mechanical and dynamic properties of a blend can be achieved by surface treatments such as grafting of functional groups on one of the blend components or activation by the application of a coating of a polymer. This paper describes the effect of grafting maleic anhydride on reclaim rubber with varying levels of maleic anhydride (i.e., 2 and 5 phr) on open two roll mills. Investigated cure characteristics and …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 1, 2017 · pp. 18–23 Read article
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A Simplified High-Performance Liquid Chromatographic Method For Determination of Vitamin D3 in Human Serum
Abstract: Diabetes is a metabolic disorder caused by defective insulin secretion, insulin action or both. The two major factors for the development of diabetes are pancreatic beta cell dysfunction and insulin resistance. In type 2 diabetes mellitus, production and release of insulin is unobstructed but due to factors like ageing or obesity, the produced insulin cannot compensate for the increased demand. Measurement of the serum level of 25-hydroxyvitamin D3 is the …
Published in International Journal of Analytical and Applied Chemistry · Vol. 3, Issue 1, 2017 · pp. 9–13 Read article